HRID1645633

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID70297

Benzenecarboperoxoic acid, 3-chloro-

C7H5ClO3

HCID294864

1,3-Dioxolane-2-methanol

C4H8O3

结构：CCC1(CCOc2ccnc(CS(=O)c3nc4ccccc4[nH]3)c2C)OCC2(CO1)OCCO2.[Na]

HCID66776196

未命名化合物

PRODUCTS

生成物

结构：Cc1c(OCC2OCCO2)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]

HCID66776143

未命名化合物

收率 17.2%

PROCEDURE

实验过程

The same procedure as in the steps (4f) to (4j) described in Example (a reprecipitation operation was not performed in oxidation step with 3-chloroperbenzoic acid) was repeated using 1,3-dioxolan-2-ylmethanol obtained in the step (66b) above to obtain the title compound (411 mg, total 17.2% yield) as a white solid.

WORKUP

后处理

customobtained in the step (66b) above