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HRID1647106

反应详情

EQUATION

反应方程式

HRID 1647106 的结构方程式

REACTANTS

反应物

4
结构：CN1CCOCC1
HCID7972

4-Methylmorpholine

C5H11NO

2 次

结构：CC(C)(C)OC(=O)NCCCC(=O)O
HCID294894

n-boc-gamma-aminobutyric acid

C9H17NO4

结构：COc1nnnc(OC)c1Cl
HCID12493616

未命名化合物

结构：Cc1ccc(S(=O)(=O)O)cc1.NCCC(=O)OCc1ccccc1
HCID13502100

4-Methylbenzene-1-sulfonic acid--benzyl beta-alaninate (1/1)

C17H21NO5S

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCCCC(=O)NCCC(=O)OCc1ccccc1
HCID19926286

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

4-(t-Butoxycarbonylamino)butyric acid in THF was activated with chlorodimethoxytriazine and N-methylmorpholine and reacted with β-alanine benzyl ester p-toluenesulphonate in the presence of N-methylmorpholine to give N-[4-(1-t-butoxyformamido)butyryl]-β-alanine benzyl ester, m.p. 54°-55° C.