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HRID1649720

反应详情

EQUATION

反应方程式

HRID 1649720 的结构方程式

REACTANTS

反应物

3
结构：[Al+3].[Cl-].[Cl-].[Cl-]
HCID6451240

未命名化合物

结构：O=C1c2ccccc2C(=O)N1CCCc1ccccc1
HCID7663529

未命名化合物

结构：COC(=O)CC(C)C(=O)Cl
HCID14403282

Methyl 4-chloro-3-methyl-4-oxobutanoate

C6H9ClO3

PRODUCTS

生成物

1
结构：COC(=O)CC(C)C(=O)c1ccc(CCCN2C(=O)c3ccccc3C2=O)cc1
HCID54211140

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCCl
溶剂HCID11

1,2-Dichloroethane

C2H4Cl2

PROCEDURE

实验过程

8.2 g (50 mmol) of 3-methoxycarbonyl-2-methyl-propionic acid chloride and 13.3 g (50 mmol) of 3-phthalimidopropyl-benzene are reacted with 26 g of aluminum chloride in 1,2-dichloroethane analogously to Example 4(a). The oil obtained crystallizes from ethanol as beige coloured crystals.

WORKUP

后处理

  1. customThe oil obtained
  2. customcrystallizes from ethanol as beige coloured crystals