Hydrochloric Acid → HCID 19854919, compound

HRID 1649840Notes

Reaction equation

HRID 1649840 reaction equation
[CH2:1]([NH2:4])[CH:2]=[CH2:3].Cl.[CH2:6]=O.[CH:8]1[CH2:12][CH:11]=[CH:10][CH:9]=1>>[CH2:1]([N:4]1[CH2:6][CH:12]2[CH2:8][CH:9]1[CH:10]=[CH:11]2)[CH:2]=[CH2:3]

Participants

5

Reactant 4

HCID 313Hydrochloric AcidHCID 712FormaldehydeHCID 7612CyclopentadieneHCID 7853Allylamine

Product 1

HCID 19854919HCID 19854919, compoundYield 91%

Procedure

According to Variant A, 144 g (2.5 moles) of allyl amine are neutralized with hydrochloric acid solution, are reacted with 187.5 g (2.5 moles) of 40% formalin solution and 198 g (3.0 moles) of cyclopentadiene, and are worked up. After vacuum distillation 313 g of a product containing 98% (V) are obtained. This corresponds to a yield of 91% of theoretical.

Workup

  1. distillationAfter vacuum distillation 313 g of a product
  2. additioncontaining 98% (V)
  3. customare obtained

Sources & evidence

ORD record
ord-d55eba9acba04c81bf286a820bbebc59
Source dataset
uspto-grants-1990_05
Patent number
US04921879

Reaction notes

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