HRID1650129
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The copper, barium, and yttrium solutions were mixed and the potassium oxalate solution was added all at once with vigorous stirring. The pH of the solution was 11.3. A brown gelatinous precipitate formed, and it was filtered, washed thoroughly with water, dried at 120° C., and crushed to a fine powder. The elemental analysis shown in the table below suggested YBa2Cu3 (OH)3 (Ox)2O3.H2O.
WORKUP
后处理
- customA brown gelatinous precipitate formed
- filtrationit was filtered
- washwashed thoroughly with water
- customdried at 120° C.
- customcrushed to a fine powder