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HRID1657589

反应详情

EQUATION

反应方程式

HRID 1657589 的结构方程式

REACTANTS

反应物

3
结构：ClCCCBr
HCID8006

1-Bromo-3-chloropropane

C3H6BrCl

结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：COc1ccc2c(c1)Nc1cccc(S(=O)(=O)N(C)C)c1S2
HCID21534844

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c(c1)N(CCCCl)c1cccc(S(=O)(=O)N(C)C)c1S2
HCID21534857

未命名化合物

收率 60.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCC(C)=O
溶剂HCID6569

Methyl ethyl ketone

C4H8O

PROCEDURE

实验过程

2-Methoxy-6-dimethylsulphamoyl-10-(3-chloropropyl)phenothiazine (m.p. 124°-126°C.; 62.6 g.) is prepared by reacting 1-bromo-3-chloropropane (147 g.) with 2-methoxy-6-dimethylsulphamoylphenothiazine (84.4 g.) in the presence of powdered potassium hydroxide (25.8 g.) in methyl ethyl ketone (300 cc.).