Hydrochloric Acid → HCID 54209856, compound

HRID 1657607Notes

Reaction equation

HRID 1657607 reaction equation
[O:1]1[CH:6]=[CH:5][CH2:4][CH2:3][CH2:2]1.[OH:7][C:8]1[CH:21]=[CH:20][C:19]2[S:18][C:17]3[C:12](=[CH:13][CH:14]=[CH:15][C:16]=3[S:22](=[O:27])(=[O:26])[N:23]([CH3:25])[CH3:24])[N:11]([CH2:28][CH2:29][CH2:30][Cl:31])[C:10]=2[CH:9]=1.Cl>C(O)C>[O:1]1[CH2:2][CH2:3][CH2:4][CH2:5][CH:6]1[O:7][C:8]1[CH:21]=[CH:20][C:19]2[S:18][C:17]3[C:12](=[CH:13][CH:14]=[CH:15][C:16]=3[S:22](=[O:26])(=[O:27])[N:23]([CH3:24])[CH3:25])[N:11]([CH2:28][CH2:29][CH2:30][Cl:31])[C:10]=2[CH:9]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 80803,4-dihydro-2H-pyranHCID 21534842HCID 21534842, compound

Product 1

HCID 54209856HCID 54209856, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

15.7 g.) is prepared by reacting dihydropyran (102 g.) with 2-hydroxy-6-dimethylsulphamoyl-10-(3-chloropropyl)-phenothiazine (17.2 g.) in the presence of an 8N solution of hydrogen chloride in ethanol (0.1 cc.).

Workup

  1. custom) is prepared

Sources & evidence

ORD record
ord-22687ae0728f4691998c0fbb2a1cb0d5
Source dataset
uspto-grants-1976_06
Patent number
US03961055

Reaction notes

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