反应详情

A mixture of 1.02 g. of 1,3-dihydrospiro[isobenzofuran-1,4'-piperidine]-3-one, 1.0 g. of sodium bicarbonate, 10 ml. of chloroform, and 0.60 g. of allyl bromide is stirred at room temperature for 24 hours and filtered. The filtrate is washed with water, dried over potassium carbonate, and concentrated to an oily solid.

1. additionA mixture of 1.02 g
2. filtrationfiltered
3. washThe filtrate is washed with water
4. dry with materialdried over potassium carbonate
5. concentrationconcentrated to an oily solid