Azobisisobutyronitrile → HCID 86738184, compound
Reaction equation
[C:1]1(=[O:7])[O:6][C:4](=[O:5])[CH:3]=[CH:2]1.[CH3:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH:14]=[CH2:15].CC(N=NC(C#N)(C)C)(C#N)C>C1(C)C=CC=CC=1>[CH2:8]=[CH:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].[C:4]1(=[O:5])[O:6][C:1](=[O:7])[CH:2]=[CH:3]1Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
98 Grams of maleic acid anhydride, 112 g of octene-1, 800 g of toluene and 4 g of AIBN were stirred for 9 hours at 90° C. Subsequently the mixture was rotated to dryness, the unreacted starting material being evaporated in the process.
Workup
- custombeing evaporated in the process
Sources & evidence
- ORD record
- ord-51d090eb9e5f4de58cee4c9d2e5d9324
- Source dataset
- uspto-grants-1981_12
- Patent number
- US04308362
Reaction notes
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