反应详情

Bromoacetophenone-modified aminopropylsilylated glass surfaces (2.5×7.5 cm; Sigma, Silane-Prep™, S4651) (see Example 13) were coated with a 0.1M solution of sodium thiocyanate in ethanol and incubated for five hours at 50° C. The glass surfaces thus treated were then washed five times using respectively 30 mL of ethanol for 3 minutes each at room temperature. After washing three times for three minutes each using respectively 30 mL of DCM at room temperature, the glass surfaces were dried and stored at 4° C. until further use.

1. additionThe glass surfaces thus treated
2. washwere then washed five times
3. customfor 3 minutes
4. customat room temperature
5. washAfter washing three times for three minutes each using respectively 30 mL of DCM at room temperature
6. customthe glass surfaces were dried
7. customstored at 4° C. until further use