2-Bromopyridine → HCID 67430077, compound

HRID 1662624Notes

Reaction equation

HRID 1662624 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][C:6](=[O:11])[C:5]2=[O:12].Br[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=1>>[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][C:6](=[O:11])[C:5]2([OH:12])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=1

Participants

3

Reactant 2

HCID 79732-BromopyridineHCID 872035-chloro-1H-indole-2,3-dione

Product 1

HCID 67430077HCID 67430077, compoundYield 35%

Procedure

With 10.0 g of 5-chloro-1H-indol-2,3-dione and 25.3 g of bromo pyridine as starting materials, 5.03 g of the title compound (orange color solid) was obtained by a similar method to Step 34-3.

Sources & evidence

ORD record
ord-9af56f20f0144b3887abce90190b7ff4
Source dataset
uspto-grants-2011_10
Patent number
US08030499B2

Reaction notes

Loading…