HRID1672055

反应详情

EQUATION

反应方程式

HRID 1672055 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of tert-butyl 1-(pyridazin-3-yl)cyclopropylcarbamate (0.3 g) in THF (3 ml) at 0° C. was added HCl in dioxane (5 ml) and the mixture stirred at r.t. for 3 hr. The reaction mixture was concentrated, and the crude product was taken for the next coupling reaction. Yield: 0.21 g

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated
  2. customthe crude product was taken for the next coupling reaction