HRID1672377
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
tert-Butyl 7-(2-chlorophenyl)-6-oxo-1,7-diazaspiro[4.4]nonane-1-carboxylate was dissolved in a 4.0 M solution of HCl in 1,4-dioxane, and the resulting mixture was stirred for 2 h at RT. The volatiles were removed in vacuo to afford the desired product, which was used in the next step without further purification. LC-MS: 251.0 (M+1H)+.
WORKUP
后处理
- customThe volatiles were removed in vacuo