HRID1673457

反应详情

EQUATION

反应方程式

HRID 1673457 的结构方程式

PROCEDURE

实验过程

3.0 mL of trifluoroacetic acid solution containing 40 mg of tert-butyl 2-(benzamido)-4-(4-nitrophenyl)benzoate was stirred at room temperature for 1 hour. The solvent was evaporated under reduced pressure and ethyl acetate and methanol were added to she obtained residue and a solid substance was separated by filtration to obtain 15 mg of 2-(benzamido)-4-(4-nitrophenyl)benzoic acid as white solid.

WORKUP

后处理

  1. customThe solvent was evaporated under reduced pressure and ethyl acetate and methanol
  2. additionwere added to she
  3. customobtained residue
  4. customa solid substance was separated by filtration