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HRID1680209

反应详情

EQUATION

反应方程式

HRID 1680209 的结构方程式

REACTANTS

反应物

4
结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：O=C1CCC(=O)N1O
HCID80170

2,5-Pyrrolidinedione, 1-hydroxy-

C4H5NO3

结构：[Br-].[K+]
HCID253877

Potassium bromide

BrK

结构：O=C(NCCCC[C@H](NC(=O)OCC(Cl)(Cl)Cl)C(=O)O)OCC(Cl)(Cl)Cl
HCID22816296

未命名化合物

PRODUCTS

生成物

1
结构：O=C1CC(OC(=O)[C@H](CCCCNC(=O)OCC(Cl)(Cl)Cl)NC(=O)OCC(Cl)(Cl)Cl)C(=O)N1
HCID22816297

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

In a manner similar to Example 2A, utilizing anhydrous ethyl acetate as the solvent, N,N'-bis-trichloroethoxycarbonyl-L-lysine is reacted with N-hydroxy succinimide to obtain the above named compound; [α]D26 -19.6° (EtOH); νmax (KBr) 1820, 1785, 1715 cm-1.

WORKUP

后处理

  1. customto obtain the above named compound