Potassium Carbonate → HCID 57099041, compound

HRID 1681134Notes

Reaction equation

HRID 1681134 reaction equation
[Cl:1][C:2]([C:12]([F:15])([F:14])[F:13])=[CH:3][C:4]1[CH:11]=[CH:10][C:7]([CH2:8]Br)=[CH:6][CH:5]=1.[C:16]([N:20]1[C:25](=[O:26])[C:24]([Cl:27])=[C:23]([SH:28])[CH:22]=[N:21]1)([CH3:19])([CH3:18])[CH3:17].C(=O)([O-])[O-].[K+].[K+]>CN(C)C=O>[C:16]([N:20]1[C:25](=[O:26])[C:24]([Cl:27])=[C:23]([S:28][CH2:8][C:7]2[CH:10]=[CH:11][C:4]([CH:3]=[C:2]([Cl:1])[C:12]([F:15])([F:14])[F:13])=[CH:5][CH:6]=2)[CH:22]=[N:21]1)([CH3:19])([CH3:17])[CH3:18]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 134692424-Chloro-2-(1,1-dimethylethyl)-5-mercapto-3(2H)-pyridazinoneHCID 537438994-(2-Chloro-3,3,3-trifluoroprop-1-enyl)-benzyl bromide

Product 1

HCID 57099041HCID 57099041, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

1.2 g of 4-(2-chloro-3,3,3-trifluoroprop-1-enyl)-benzyl bromide and 0.8 g of 2-tert.-butyl-4-chloro-5-mercapto-3(2H)-pyridazinone are added to a suspension of 0.7 g of potassium carbonate in 10 cc of dimethylformamide.

Sources & evidence

ORD record
ord-29b3fb0556904bbdae97436b1c3e550e
Source dataset
uspto-grants-1992_12
Patent number
US05169848

Reaction notes

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