反应详情

温度

225 °C

A mixture of 2-amino-6-chloropyridine in 100 mL of morpholine was heated at 225° C. for 60 mins. The mixture was cooled and precipitate filtered off, the filtrate was concentrated to give the 17 gram product as a brown oil.

1. temperatureThe mixture was cooled
2. filtrationprecipitate filtered off
3. concentrationthe filtrate was concentrated