反应详情

2-Picolyl chloride hydrochloride (3.03 g) was added to a stirred suspension of 3-chloro-4-fluorobenzenethiol (3.0 g) and cesium carbonate (12.0 g) in DMF (50 ml) and the mixture stirred at RT overnight. Mixture poured into water, organics extracted into ether and the ether extracts washed (brine), dried (MgSO4) and evaporated under reduced pressure to a green oil (4.0 g).

1. extractionorganics extracted into ether
2. washthe ether extracts washed (brine)
3. dry with materialdried (MgSO4)
4. customevaporated under reduced pressure to a green oil (4.0 g)