Methylamine → HCID 11591342, compound

HRID 1689744Notes

Reaction equation

HRID 1689744 reaction equation
[CH3:1][NH:2][C:3]([C:5]1[C:10]([NH2:11])=[C:9]([NH:12][C:13]2[CH:17]=[C:16]([CH3:18])[NH:15][N:14]=2)[N:8]=[C:7]([S:19][C:20]2[CH:25]=[CH:24][C:23]([NH:26][C:27]([CH:29]3[CH2:31][CH2:30]3)=[O:28])=[CH:22][CH:21]=2)[N:6]=1)=[O:4].CN.[CH3:34][N:35]([CH2:37]CN)[CH3:36]>>[CH3:34][N:35]([CH2:37][CH2:1][NH:2][C:3]([C:5]1[C:10]([NH2:11])=[C:9]([NH:12][C:13]2[CH:17]=[C:16]([CH3:18])[NH:15][N:14]=2)[N:8]=[C:7]([S:19][C:20]2[CH:25]=[CH:24][C:23]([NH:26][C:27]([CH:29]3[CH2:31][CH2:30]3)=[O:28])=[CH:22][CH:21]=2)[N:6]=1)=[O:4])[CH3:36]

Participants

4

Reactant 3

HCID 6329MethylamineHCID 66053N,N-DimethylethylenediamineHCID 11690693HCID 11690693, compound

Product 1

HCID 11591342HCID 11591342, compound

Procedure

The title compound was prepared in the manner described above for compound 9 with the exception that the methylamine reagent was replaced with 2-(N,N-dimethylamino)ethylamine. The title compound was recovered as a yellow-off white solid.

Workup

  1. customThe title compound was recovered as a yellow-off white solid

Sources & evidence

ORD record
ord-561d27633849491eb8f666ed29e819d1
Source dataset
uspto-grants-2012_04
Patent number
US08153630B2

Reaction notes

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