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HRID1691595

反应详情

EQUATION

反应方程式

HRID 1691595 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=[N+]([O-])c1cnc(Cl)c([N+](=O)[O-])c1
HCID75738

Pyridine, 2-chloro-3,5-dinitro-

C5H2ClN3O4

结构：CC(C)(C)OC(=O)CCCN.Cl
HCID24750478

tert-Butyl 4-aminobutanoate--hydrogen chloride (1/1)

C8H18ClNO2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)CCCNc1ncc([N+](=O)[O-])cc1[N+](=O)[O-]
HCID86643266

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

CONDITIONS

反应条件

温度
60 °C

PROCEDURE

实验过程

A suspension of 3 g (14.74 mmol) of 2-chloro-3,5-dinitropyridine in dioxane is admixed with 3.46 g (17.69 mmol) of tert-butyl 4-aminobutanoate hydrochloride and then with 4.21 ml (22.11 mmol) of triethylamine. The reaction mixture is stirred at 60° C. for 3 hours.