Hydrochloric Acid → HCID 87336768, compound
Reaction equation
[CH3:1][C:2]1[C:7]2[C:8]([O:10][C:11]3[C:12]([CH3:23])=[C:13]([O:21][CH3:22])[CH:14]=[C:15]([C:18]([OH:20])=[O:19])[C:16]=3[O:17][C:6]=2[C:5]([CH:24]=[O:25])=[C:4]([OH:26])[CH:3]=1)=[O:9].Cl.[OH-:28].[Li+]>>[CH3:1][C:2]1[C:7]([C:8]([OH:9])=[O:28])=[C:6]([O:17][C:16]2[C:15]([C:18]([OH:20])=[O:19])=[CH:14][C:13]([O:21][CH3:22])=[C:12]([CH3:23])[C:11]=2[OH:10])[C:5]([CH:24]=[O:25])=[C:4]([OH:26])[CH:3]=1Participants
4
Procedure
Psoromic acid (35 mg, 1 mmol) was dissolved in 1 mol/L of aqueous lithium hydroxide (3 ml), and the reaction is allowed to stand overnight. The solution was acidified to a pH of 4 with 1 mol/L dilute HCl, filtered, and collected to give a white solid product.
Workup
- filtrationfiltered
- customcollected
- customto give a white solid product
Sources & evidence
- ORD record
- ord-4c44f4b558cd4225b24c19a0ce733331
- Source dataset
- uspto-grants-2012_04
- Patent number
- US08158623B2
Reaction notes
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