Triethylamine → HCID 57960743, compound

HRID 1695555Notes

Reaction equation

HRID 1695555 reaction equation
[CH3:1][O:2][CH2:3][C@@H:4]([NH2:6])[CH3:5].Cl[C:8]([O:10][CH2:11][CH3:12])=[O:9].C(N(CC)CC)C>O1CCCC1>[CH2:11]([O:10][C:8](=[O:9])[NH:6][C@@H:4]([CH3:5])[CH2:3][O:2][CH3:1])[CH3:12]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 10928Ethyl chloroformateHCID 70215362-Propanamine, 1-methoxy-, (2S)-

Product 1

HCID 57960743HCID 57960743, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

A solution of (S)-1-methoxy-2-propylamine in tetrahydrofuran was allowed to undergo the reaction with ethyl chloroformate in the presence of triethylamine to obtain [(1S)-2-methoxy-1-methylethyl]carbamic acid ethyl ester.

Sources & evidence

ORD record
ord-d085f5b1189b4351a45b494610d2486d
Source dataset
uspto-grants-2012_04
Patent number
US08163746B2

Reaction notes

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