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HRID1697714

反应详情

EQUATION

反应方程式

HRID 1697714 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)CC(=O)OC(C)(C)C
HCID15538

tert-Butyl 3-oxobutanoate

C8H14O3

结构：COC(=O)[C@@H]1C[C@@H](S(=O)(=O)CC2CC2)CN1.O=C(O)C(F)(F)F
HCID66770846

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)[C@@H]1C[C@@H](S(=O)(=O)CC2CC2)CN1C(=O)CC(C)=O
HCID86646863

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

In analogy to the procedure described in example 192f, (2S,4R)-4-cyclopropylmethanesulfonyl-pyrrolidine-2-carboxylic acid methyl ester trifluoroacetate was reacted with tert-butyl acetoacetate in the presence of triethylamine to give the title compound as brown solid. MS (ESI): m/z=332.2 [M+H]+.