HRID1699341

反应详情

EQUATION

反应方程式

HRID 1699341 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

On the other hand, magnesium aluminate metasilicate was dispersed in water as inorganic fine particles together with a very small amount of a surfactant (Surfinol 440, mfd. by Nissin Kagaku Kogyo K.K.), and the resulting dispersion, methyl methacrylate, butyl methacrylate, butyl acrylate and 3-trimethoxysilylpropyl methacrylate were mixed in the weight ratio of 3:2:3:2:0.2. The resulting mixture was treated with nitrogen to replace the air, after which potassium persulfate was added and emulsion polymerization was carried out at 60° C. for 8 hours. After completion of the reaction, the concentration was adjusted with water to prepare an (inorganic fine particles)-coated organic fine particles dispersion F (40 wt %) in which magnesium aluminate metasilicate fine particles had been formed on the surfaces of the acrylic copolymer resin fine particles.

WORKUP

后处理

  1. additionThe resulting mixture was treated with nitrogen
  2. customemulsion polymerization
  3. customAfter completion of the reaction
  4. concentrationthe concentration
  5. customto prepare an (inorganic fine particles)-coated organic fine particles dispersion F (40 wt %) in which magnesium aluminate metasilicate fine particles