反应详情

To 69.5 ml. of 1 molar borane in tetrahydrofuran chilled in an ice bath is added dropwise over 40 minutes a solution of 17.2 g. of p-decylbenzoic acid in 150 ml. of dry tetrahydrofuran. The mixture is refluxed for 3.5 hours, chilled, 5 ml. of concentrated hydrochloric acid is added and the mixture poured onto ice. The mixture is filtered and the solid washed with water to give white crystals.

1. additionis added dropwise over 40 minutes a solution of 17.2 g
2. temperatureThe mixture is refluxed for 3.5 hours
3. temperaturechilled
4. additionthe mixture poured onto ice
5. filtrationThe mixture is filtered
6. washthe solid washed with water
7. customto give white crystals