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HRID1703913

反应详情

EQUATION

反应方程式

HRID 1703913 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：NCc1ccccc1Cl
HCID66648

2-Chlorobenzylamine

C7H8ClN

结构：CC(=O)c1ccc(Cl)c(S(=O)(=O)Cl)c1
HCID12619795

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)c1ccc(Cl)c(S(=O)(=O)NCc2ccccc2Cl)c1
HCID22760412

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

25.5 g of 4'-chloro-3'-chlorosulfonylacetophenone were reacted with 16 g of o-chloro-benzyl amine and 25.5 g of triethyl amine and worked up. Colorless crystals from isopropanol (active charcoal), melting point: 102° C.