2-Acetylhydroquinone → HCID 14983041, compound

HRID 1708701Notes

Reaction equation

HRID 1708701 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[CH:12]1([C:18](Cl)=O)[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1.Br[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26]Cl.[OH:28][CH:29]1[CH2:34][CH2:33][NH:32][CH2:31][CH2:30]1>>[CH:12]1([C:18]2[O:1][C:2]3[CH:7]=[CH:6][C:5]([O:8][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][N:32]4[CH2:33][CH2:34][CH:29]([OH:28])[CH2:30][CH2:31]4)=[CH:4][C:3]=3[C:9](=[O:11])[CH:10]=2)[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17]1

Participants

5

Reactant 4

HCID 102792-AcetylhydroquinoneHCID 75938Cyclohexanecarbonyl chlorideHCID 79341Piperidin-4-olHCID 960701-Bromo-5-chloropentane

Product 1

HCID 14983041HCID 14983041, compound

Procedure

The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, cyclohexanecarbonyl chloride, 1-bromo-5-chloropentane, and 4-hydroxypiperidine: mp 85°-86° C.

Sources & evidence

ORD record
ord-e978d94bbdb84c28a1bcf0546c00301b
Source dataset
uspto-grants-1994_10
Patent number
US05359098

Reaction notes

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