2-Acetylhydroquinone → HCID 18959691, compound

HRID 1708717Notes

Reaction equation

HRID 1708717 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[CH:12]1([C:16]([Cl:18])=O)[CH2:15][CH2:14][CH2:13]1.Br[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25]Cl.[OH:27][CH:28]1[CH2:33][CH2:32][NH:31][CH2:30][CH2:29]1>>[ClH:18].[CH:12]1([C:16]2[O:1][C:2]3[CH:7]=[CH:6][C:5]([O:8][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][N:31]4[CH2:32][CH2:33][CH:28]([OH:27])[CH2:29][CH2:30]4)=[CH:4][C:3]=3[C:9](=[O:11])[CH:10]=2)[CH2:13][CH2:14][CH2:15]1

Participants

5

Reactant 4

HCID 102792-AcetylhydroquinoneHCID 78705Cyclobutanecarbonyl chlorideHCID 79341Piperidin-4-olHCID 805161-Bromo-6-chlorohexane

Product 1

HCID 18959691HCID 18959691, compound

Procedure

The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, cyclobutanecarbonyl chloride, 1-bromo-6-chlorohexane, and 4-hydroxypiperidine: mp 111°-113° C.

Sources & evidence

ORD record
ord-85fde987026b449b961d78b3e4577a30
Source dataset
uspto-grants-1994_10
Patent number
US05359098

Reaction notes

Loading…