2-Acetylhydroquinone → HCID 18959682, compound

HRID 1708720Notes

Reaction equation

HRID 1708720 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[S:12]1[CH:16]=[CH:15][CH:14]=[C:13]1[C:17]([Cl:19])=O.Br[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26]Cl.[OH:28][CH:29]1[CH2:34][CH2:33][NH:32][CH2:31][CH2:30]1>>[ClH:19].[OH:28][CH:29]1[CH2:34][CH2:33][N:32]([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][O:8][C:5]2[CH:6]=[CH:7][C:2]3[O:1][C:17]([C:13]4[S:12][CH:16]=[CH:15][CH:14]=4)=[CH:10][C:9](=[O:11])[C:3]=3[CH:4]=2)[CH2:31][CH2:30]1

Participants

5

Reactant 4

HCID 102792-AcetylhydroquinoneHCID 789282-Thiophenecarbonyl chlorideHCID 79341Piperidin-4-olHCID 805161-Bromo-6-chlorohexane

Product 1

HCID 18959682HCID 18959682, compound

Procedure

The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, 2-thiophenecarbonyl chloride, 1-bromo-6-chlorohexane, and 4-hydroxypiperidine: mp 211°-212° C.

Sources & evidence

ORD record
ord-d68b5ddd14d24b678be9c3e7b5b05170
Source dataset
uspto-grants-1994_10
Patent number
US05359098

Reaction notes

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