HRID1713139

反应详情

EQUATION

反应方程式

HRID 1713139 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of ethyl pyrido[3,4-b]pyrazine-6(5H)-carboxylate (149 mg, 0.726 mmol) in EtOAc (25 mL) is added 10% Pd/C (100 mg). The mixture is hydrogenated at 30 psi. overnight. The mixture is filtered through Celite and the solvent removed under vacuum to yield the title compound. MS (+VE) m/z 208.16 (M++1).

WORKUP

后处理

  1. customovernight
  2. filtrationThe mixture is filtered through Celite
  3. customthe solvent removed under vacuum