Quinizarin → Anthraquinone, 1,4-bis((2-morpholinoethyl)amino)-

HRID 1719470Notes

Reaction equation

HRID 1719470 reaction equation
[CH:1]1[CH:2]=[CH:3][C:4]2[C:15](=[O:16])[C:14]3[C:9](=[C:10](O)[CH:11]=[CH:12][C:13]=3O)[C:7](=[O:8])[C:5]=2[CH:6]=1.[NH2:19][CH2:20][CH2:21][N:22]1[CH2:27][CH2:26][O:25][CH2:24][CH2:23]1>O>[O:25]1[CH2:26][CH2:27][N:22]([CH2:21][CH2:20][NH:19][C:10]2[C:9]3[C:7](=[O:8])[C:5]4[C:4](=[CH:3][CH:2]=[CH:1][CH:6]=4)[C:15](=[O:16])[C:14]=3[C:13]([NH:19][CH2:20][CH2:21][N:22]3[CH2:27][CH2:26][O:25][CH2:24][CH2:23]3)=[CH:12][CH:11]=2)[CH2:23][CH2:24]1

Participants

4

Reactant 2

HCID 6688QuinizarinHCID 4082852-Morpholinoethylamine

Product 1

HCID 72737Anthraquinone, 1,4-bis((2-morpholinoethyl)amino)-

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A 9.60 g. portion of quinizarin, 46.90 g. of N-(2-aminoethyl)morpholine and 56 ml. of water are reacted as described in Example 1 giving 9.92 g. of the desired product as a blue-black solid, mp. 158°-159° C.

Sources & evidence

ORD record
ord-5b0d80eb0b654f0cb46699fe1a81a01d
Source dataset
uspto-grants-1985_09
Patent number
US04540583

Reaction notes

Loading…