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HRID1720030

反应详情

EQUATION

反应方程式

HRID 1720030 的结构方程式

REACTANTS

反应物

2
结构：O=S([O-])[O-].[Na+].[Na+]
HCID24437

Sodium sulfite

Na2O3S

结构：O=[N+]([O-])c1cc(F)ccc1CBr
HCID12761379

1-(Bromomethyl)-4-fluoro-2-nitrobenzene

C7H5BrFNO2

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cc(F)ccc1CS(=O)(=O)[O-].[Na+]
HCID86749374

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A solution of 4-fluoro-2-nitrobenzylbromide (50.1 g) and sodium sulfite (27.3 g) in water (200 ml) was heated under reflux for 2.5 hours and cooled to room temperature. The solvent was removed under reduced pressure and ethanol (100 ml) was added to the crude product.

WORKUP

后处理

  1. temperatureunder reflux for 2.5 hours
  2. customThe solvent was removed under reduced pressure and ethanol (100 ml)
  3. additionwas added to the crude product