Isobutanol → HCID 18669862, compound

In a sufficiently dried egg-plant type flask provided with a stirrer was charged 0.148 g (2 mmol) of sufficiently purified isobutanol, which was sufficiently dried. After completion of the drying, 3.3 ml of methylene chloride was added thereto. Then, under nitrogen atmosphere, 0.9 ml (1 mmol) of trimethylaluminum was slowly added dropwise with ice-cooling and stirring, and the mixture was mixed in the dark at room temperature for 1 hour to obtain a methylene chloride solution of methylaluminum bis(isobutoxide) (1 mmol/3.3 ml).

1. customIn a sufficiently dried egg-plant type flask provided with a stirrer
2. customwas sufficiently dried
3. additionAfter completion of the drying, 3.3 ml of methylene chloride was added
4. temperaturecooling
5. additionthe mixture was mixed in the dark at room temperature for 1 hour

ORD record

ord-0aaa55ecb7c44f6b8e900506cb0ea90a

Source dataset

uspto-grants-1994_07

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US05328970