HRID1730101

反应详情

EQUATION

反应方程式

HRID 1730101 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1-Chloro-amitriptyline (196 mg) in 3 ml. absolute ethanol was added to an ethanolic solution of 1.1 eq. d-tartaric acid and warmed for 5-10 mins. The title compound was precipitated with ethyl ether as a white powder. After purity and identification checks, the overall yield from amitriptyline base was 32%.

WORKUP

后处理

  1. temperaturewarmed for 5-10 mins
  2. customThe title compound was precipitated with ethyl ether as a white powder