HRID1730178

反应详情

EQUATION

反应方程式

HRID 1730178 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The above compound is prepared by refluxing 8 gm. of 2-(2-amino-5-thiadiazolyl)-1-methyl-5-nitroimidazole in 30 ml. of 98% formic acid for 10 hours, cooling, and adding the mixture to saturated sodium bicarbonate solution, and the solid collected. The compound melts at 225° to 227° C.

WORKUP

后处理

  1. customThe above compound is prepared
  2. temperatureby refluxing 8 gm
  3. temperaturecooling
  4. customthe solid collected