2-Amino-2',5-dichlorobenzophenone → 2-Amino-2',5-dichlorobenzophenone hydrazine

HRID 1730451Notes

Reaction equation

HRID 1730451 reaction equation
[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12])=[O:5].O.[NH2:19][NH2:20]>C(O)COCCO>[NH2:19][NH2:20].[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12])=[O:5]

Participants

4

Reactant 2

HCID 180692-Amino-2',5-dichlorobenzophenoneHCID 24654Hydrazine hydrate (1:1)

Product 1

HCID 214973892-Amino-2',5-dichlorobenzophenone hydrazine

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

In the manner given in Preparation 1, 2-amino-2',5-dichlorobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 2-amino-2',5-dichlorobenzophenone hydrazine.

Sources & evidence

ORD record
ord-b4517f0ac9e846239e92541d982583ed
Source dataset
uspto-grants-1976_11
Patent number
US03992400

Reaction notes

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