Furfurylamine → HCID 54410215, compound

HRID 1733238Notes

Reaction equation

HRID 1733238 reaction equation
O=[CH:2][C@@H:3]([C@H:5]([C@H:7]([C@@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4].[CH2:13]([NH2:19])[C:14]1[O:18][CH:17]=[CH:16][CH:15]=1.[Cl:20][CH2:21][CH2:22][N:23]=[C:24]=[O:25]>>[Cl:20][CH2:21][CH2:22][NH:23][C:24]([N:19]([CH2:13][C:14]1[O:18][CH:17]=[CH:16][CH:15]=1)[CH:2]1[O:10][C@H:9]([CH2:11][OH:12])[C@H:7]([OH:8])[C@H:5]([OH:6])[C@H:3]1[OH:4])=[O:25]

Participants

4

Reactant 3

HCID 3438FurfurylamineHCID 160352-Chloroethyl isocyanateHCID 3037556(2R,3S,4S,5R)-2,3,4,5,6-pentahydroxyhexanal

Product 1

HCID 54410215HCID 54410215, compoundYield 60.2%

Procedure

5.5 g of D-galactose, 3.8 g of furfurylamine and 3.5 g of 2-chloroethyl isocyanate are treated in the same manner as described in Example 23-(1). 6.7 g of 1-(2-chloroethyl)-3-furfuryl-3-(D-galactopyranosyl)urea are thereby obtained as colorless powder.

Sources & evidence

ORD record
ord-8e1e902586824ed79370a19a0471edc4
Source dataset
uspto-grants-1980_12
Patent number
US04241052

Reaction notes

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