Potassium Carbonate → HCID 1474903, compound

HRID 1735086Notes

Reaction equation

HRID 1735086 reaction equation
[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]([CH:11]=O)=[C:3]1Cl.C([O-])([O-])=O.[K+].[K+].[SH:20][CH2:21][C:22]([O:24][CH3:25])=[O:23]>>[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]2[CH:11]=[C:21]([C:22]([O:24][CH3:25])=[O:23])[S:20][C:3]1=2

Participants

4

Reactant 3

HCID 11430Potassium CarbonateHCID 16907Methyl ThioglycolateHCID 3147922-Chloro-1-methyl-1H-indole-3-carbaldehyde

Product 1

HCID 1474903HCID 1474903, compound

Procedure

Prepared from (3) (9.6 g), K2CO3 (15 g) and methyl 2-mercaptoacetate (10 ml) yielding (6) (9.3 g), m.p. 133.5°-133.8° C.

Sources & evidence

ORD record
ord-b07b8702eeaa4be6aa62832621e4b8a1
Source dataset
uspto-grants-1996_07
Patent number
US05536721

Reaction notes

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