Potassium Carbonate → HCID 19068988, compound

HRID 1735087Notes

Reaction equation

HRID 1735087 reaction equation
[CH:1]1([CH2:4][N:5]2[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[C:7]([CH:14]=O)=[C:6]2Cl)[CH2:3][CH2:2]1.C([O-])([O-])=O.[K+].[K+].[SH:23][CH2:24][C:25]([O:27][CH3:28])=[O:26]>>[CH:1]1([CH2:4][N:5]2[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[C:7]3[CH:14]=[C:24]([C:25]([O:27][CH3:28])=[O:26])[S:23][C:6]2=3)[CH2:2][CH2:3]1

Participants

4

Reactant 3

HCID 11430Potassium CarbonateHCID 16907Methyl ThioglycolateHCID 12643608HCID 12643608, compound

Product 1

HCID 19068988HCID 19068988, compound

Procedure

Prepared from (4) (6.5 g), K2CO3 (10 g) and methyl 2-mercaptoacetate (3.2 ml) yielding (7) (6 g), m.p. 110°-111° C.

Sources & evidence

ORD record
ord-4f33aeec91d248478a0ec78442188300
Source dataset
uspto-grants-1996_07
Patent number
US05536721

Reaction notes

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