Potassium Carbonate → HCID 19068934, compound

HRID 1735101Notes

Reaction equation

HRID 1735101 reaction equation
[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][C:7]([CH3:11])=[CH:8][CH:9]=2)[C:4]([CH:12]=O)=[C:3]1Cl.C([O-])([O-])=O.[K+].[K+].[SH:21][CH2:22][C:23]([O:25][CH3:26])=[O:24]>>[CH3:11][C:7]1[CH:6]=[C:5]2[C:10](=[CH:9][CH:8]=1)[N:2]([CH3:1])[C:3]1[S:21][C:22]([C:23]([O:25][CH3:26])=[O:24])=[CH:12][C:4]2=1

Participants

4

Reactant 3

HCID 11430Potassium CarbonateHCID 16907Methyl ThioglycolateHCID 19068972HCID 19068972, compound

Product 1

HCID 19068934HCID 19068934, compoundYield 14.4%

Procedure

Prepared from (46) (0.80 g), K2CO3 (1.5 g) and methyl 2-mercaptoacetate (0.60 ml) yielding (52) 0.144 g (14.4%). M.p. 152°-155° C.

Sources & evidence

ORD record
ord-f7ed5986bede4adfb235d3d47f2c0cc8
Source dataset
uspto-grants-1996_07
Patent number
US05536721

Reaction notes

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