Isopropanol → HCID 9843246, compound

HRID 1735691Notes

Reaction equation

HRID 1735691 reaction equation
C([O:3][P:4]([CH2:9][CH2:10][CH2:11][N:12]([CH2:21][C:22]1[CH:27]=[CH:26][C:25]([Cl:28])=[CH:24][CH:23]=1)[CH2:13][C:14]1[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][CH:15]=1)(=[O:8])[O:5]CC)C.C(O)(C)C>Cl>[Cl:28][C:25]1[CH:24]=[CH:23][C:22]([CH2:21][N:12]([CH2:11][CH2:10][CH2:9][P:4](=[O:3])([OH:5])[OH:8])[CH2:13][C:14]2[CH:15]=[CH:16][C:17]([Cl:20])=[CH:18][CH:19]=2)=[CH:27][CH:26]=1

Participants

4

Reactant 2

HCID 3776IsopropanolHCID 54511558HCID 54511558, compound

Product 1

HCID 9843246HCID 9843246, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

3-[N,N-bis-(4-chlorobenzyl)amino]propyl phosphonic acid diethyl ester (prepared according to Example 1) was dissolved in 8N HCl (25 ml), then a small amount of isopropyl alcohol added to effect solution. After heating for 6 hours, evaporation gave the title compound as a glass.

Workup

  1. temperatureAfter heating for 6 hours
  2. customevaporation

Sources & evidence

ORD record
ord-229c753085704f6c97096d55b467de2e
Source dataset
uspto-grants-1996_07
Patent number
US05538956

Reaction notes

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