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HRID1735730

反应详情

EQUATION

反应方程式

HRID 1735730 的结构方程式

REACTANTS

反应物

2
结构：ClCCCN1CCN(c2ccccc2)CC1
HCID139197

Piperazine, 1-(3-chloropropyl)-4-phenyl-

C13H19ClN2

结构：COC(=O)C1Sc2ccccc2OCC1=O
HCID13803747

未命名化合物

PRODUCTS

生成物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：COC(=O)C1Sc2ccccc2OC(CCCN2CCN(c3ccccc3)CC2)C1=O
HCID19434348

未命名化合物

PROCEDURE

实验过程

Methyl 3-oxo-3,4-dihydro-2H-1,5-benzoxathiepine-4-carboxylate was condensed with 3-(4-phenylpiperazin-1-yl)propyl chloride in the same manner as in Reference Example 1 to isolate methyl 3-oxo-[3-(4-phenylpiperazin-1-yl)propyl]-3,4-dihydro-2H-1,5-benzoxathiepine-4-carboxylate as hydrochloride. Recrystallization from methanol yielded white crystals, melting point 176°-178° C.