HRID1742610

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID31297

Methanesulfonyl chloride

CH3ClO2S

结构：CN(C)P(=O)(N(C)C)N(C)C.CN(C)P(=O)(N(C)C)N(C)C

HCID20187980

未命名化合物

HCID131718645

未命名化合物

PRODUCTS

生成物

HCID17824068

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

结构：[Cl][Pd][Cl].c1ccc(P(c2ccccc2)c2ccccc2)cc1.c1ccc(P(c2ccccc2)c2ccccc2)cc1

催化剂HCID6102075

未命名化合物

溶剂HCID22180045

未命名化合物

PROCEDURE

实验过程

TEA - triethylamine; HMPA - hexamethylphosphoramide; THF - tetrahydrofuran; MSC - methanesulphonyl chloride; BTPC - bis(triphenylphosphine)palladium (II) chloride; DMA - dimethylamine; IMS - industrial methylated spirits; SPC - Short path chromatography carried out on silica (Merck 7747) unless otherwise stated. FCC - Flash column chromatography carried out on silica (Merck 9385). `Dried` refers to drying using sodium sulphate or magnesium sulphate unless otherwise stated.

WORKUP

后处理

custom`Dried`
customto drying