huagongshe.com
HRID1746508

反应详情

EQUATION

反应方程式

HRID 1746508 的结构方程式

REACTANTS

反应物

4
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CC(=O)Oc1ccccc1C=CC(=O)O
HCID41486

未命名化合物

结构：CCN=C=NCCCN(C)C.Cl
HCID2723939

1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride

C8H18ClN3

结构：COC(=O)[C@@H](N)Cc1ccc(OC)cc1.Cl
HCID69612215

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)[C@H](Cc1ccc(OC)cc1)NC(=O)C=Cc1ccccc1OC(C)=O
HCID86655464

未命名化合物

收率 68%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The same procedures as in Example 2 were carried out from the compound obtained in Example 33 (8.0 g), triethylamine (5.4 mL), 2-acetoxycinnamic acid (8.1 g), WSC.HCl (7.5 g), and methylene chloride (200 mL), to give the captioned compound (8.8 g, 68%) as crystals.