Guaiacol → HCID 20056858, compound

HRID 1753667Notes

Reaction equation

[C:1]1([O:8][CH3:9])[C:2](=[CH:4][CH:5]=[CH:6][CH:7]=1)[OH:3].C(=O)(O)O.[OH:14][CH2:15][CH:16]([CH2:18][OH:19])[OH:17].C(=O)([O-])[O-].[K+].[K+]>>[C:15]([O:3][C:2]1[C:1]([O:8][CH3:9])=[CH:7][CH:6]=[CH:5][CH:4]=1)(=[O:14])[CH:16]([CH2:18][OH:19])[OH:17]

Participants

Reactant 3

HCID 460Guaiacol

HCID 11430Potassium Carbonate

HCID 22377413HCID 22377413, compound

Product 1

HCID 20056858HCID 20056858, compound

Conditions

Temperature: 185 °C

Procedure

Guaiacol (249 grams), glycerine carbonate (254 grams) and potassium carbonate (1 gram) were combined and heated to 185° C. over a 6 hour period to result in a guaiacol mono-glycerate product.

Sources & evidence

ORD record: ord-1a9981a3ce88486baf56222b0fd104b1
Source dataset: uspto-grants-2015_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09164409B2

Reaction notes

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