反应详情

A solution was prepared by combining 15 g of (4-hydroxyphenyl) phenyl sulfide which had been synthesized according to the well-known formulation, 11 g of 1-bromohexane, 9 g of potassium carbonate, and 30 g of DMF. The solution was aged at 80° C. for 16 hours. The aged solution was cooled to room temperature, to which 30 g of water was added to quench the reaction. To the solution, 50 g of toluene was added for extraction. The organic layer was separated and washed with sodium hydroxide aqueous solution and water in sequence. On subsequent concentration in vacuum, 16 g of the target compound, (4-hexyloxyphenyl) phenyl sulfide was obtained as oily matter. Yield 90%.

1. customA solution was prepared
2. customhad been synthesized
3. additionwas added
4. customto quench
5. customthe reaction
6. customThe organic layer was separated
7. washwashed with sodium hydroxide aqueous solution and water in sequence
8. concentrationOn subsequent concentration in vacuum, 16 g of the target compound