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HRID1757233

反应详情

EQUATION

反应方程式

HRID 1757233 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)O)cc1.O
HCID521998

4-Methylbenzenesulfonic acid hydrate

C7H10O4S

结构：OC1CCCNC1c1ccccc1
HCID18782643

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(S(=O)(=O)[O-])cc1.O[C@H]1CCC[NH2+][C@H]1c1ccccc1
HCID86748915

未命名化合物

PROCEDURE

实验过程

The mixture of cis- and trans-isomers of 3-hydroxy-2-phenylpiperidine (Description 1, (2b)) and 4-toluenesulfonic acid monohydrate was crystallized from methanol/ethyl acetate to give cis-3-hydroxy-2-phenylpiperidinium tosylate: mp 266°-267° C.

WORKUP

后处理

  1. customwas crystallized from methanol/ethyl acetate