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HRID1757910

反应详情

EQUATION

反应方程式

HRID 1757910 的结构方程式

REACTANTS

反应物

4
反应SMILES：O
HCID962

Water

H2O

反应SMILES：O=[N+]([O-])c1ccc(O)c([N+](=O)[O-])c1
HCID1493

2,4-Dinitrophenol

C6H4N2O5

反应SMILES：OCC(Br)CBr
HCID7281

2,3-Dibromopropanol

C3H6Br2O

反应SMILES：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

PRODUCTS

产物

1
反应SMILES：O=[N+]([O-])c1ccc(OCC(CO)Oc2ccc([N+](=O)[O-])cc2[N+](=O)[O-])c([N+](=O)[O-])c1
HCID20510281

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CN(C)C=O
溶剂HCID6228

Dimethylformamide

C3H7NO

PROCEDURE

实验过程

A mixture of 19.2 gm (0.1 mol) of 2,4-dinitrophenol (96%), 13.6 gm (0.05 mol) of 2,3-dibromopropanol, and 6.9 gm (0.05 mol) of potassium carbonate was refluxed for eight hours in 20 ml of dimethylformamide. After cooling, the solution was poured into 1.5 liters of water, and the precipitated product was removed by suction and washed with water. The intermediate obtained melted with decomposition at 129° C.

WORKUP

后处理

  1. temperatureAfter cooling
  2. customthe precipitated product was removed by suction
  3. washwashed with water
  4. customThe intermediate obtained
  5. custommelted with decomposition at 129° C.