Sorbitol → HCID 67020547, compound

HRID 1758033Notes

Reaction equation

[OH:1][CH2:2][C@@H:3]([C@H:5]([C@@H:7]([C@@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4].[Cl:13][C:14]1[CH:15]=[C:16]([CH:19]=[CH:20][C:21]=1[Cl:22])[CH:17]=O>>[Cl:13][C:14]1[CH:15]=[C:16]([CH:19]=[CH:20][C:21]=1[Cl:22])[CH:17]=[C:2]([OH:1])[C@@H:3]([OH:4])[C@@H:5]([OH:6])[C@H:7]([OH:8])[C@@H:9]([OH:10])[C:11](=[CH:17][C:16]1[CH:19]=[CH:20][C:21]([Cl:22])=[C:14]([Cl:13])[CH:15]=1)[OH:12]

Participants

Reactant 2

HCID 5780Sorbitol

HCID 227103,4-Dichlorobenzaldehyde

Product 1

HCID 67020547HCID 67020547, compound

Procedure

Bis(3,4-dichlorobenzylidene)sorbitol was prepared from aqueous sorbitol and 3,4-dichlorobenzaldehyde according to the method of Example 1. The melting point of the product was 270° C.

Workup

customwas 270° C.

Sources & evidence

ORD record: ord-f4c4f9985cd3473992cac0cc09b05699
Source dataset: uspto-grants-1983_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04371645

Reaction notes

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