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HRID1759519

反应详情

EQUATION

反应方程式

HRID 1759519 的结构方程式

REACTANTS

反应物

3
结构：Cc1cc(O)c(C(C)(C)C)cc1Sc1cc(C(C)(C)C)c(O)cc1C
HCID7308

4,4'-Thiobis(6-tert-butyl-m-cresol)

C22H30O2S

结构：O=C(OO)c1cccc(Cl)c1
HCID70297

Benzenecarboperoxoic acid, 3-chloro-

C7H5ClO3

结构：CC(C)NC(=O)C(=O)C=Cc1cccc(Cl)c1
HCID53986957

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)NC(=O)C1OC1c1cccc(Cl)c1
HCID13041335

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCCl
溶剂HCID11

1,2-Dichloroethane

C2H4Cl2

PROCEDURE

实验过程

This compound was prepared from N-(1-methylethyl)-3-chlorocinnamoylcarboxamide (22.4 g.), m-chloroperbenzoic acid (23.6 g.), 4,4'-thiobis(6-tert-butyl-m-cresol) (0.3 g.), and ethylene dichloride as described in Example 7, and purified by recrystallization from ether. The compound melted at 131°-133°, and weighed 14.5 g.

WORKUP

后处理

  1. custompurified by recrystallization from ether